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>瀏覽次數(shù)：0次</span></p><a rel="nofollow" class="button">聯(lián)系我們</a></div></div><div id="pm8qhop" class="rightbox"><h3>公司基本資料信息</h3><p style="border:0;"><a rel="nofollow">上海北倉化工科技有限公司</a></p><p><span>聯(lián)系人：</span>王金良</p><p><span>郵箱: </span>shbeicang@vip.126.com</p><p><span>電話: </span>18516286991</p><p><span>傳真: </span>021_</p><p><span>網址: </span>http://www.shbeicang.cn</p><p><span>手機: </span>021-60459206</p><p><span>地址: </span>金山大道4168號</p><p>[當前離線] <a rel="nofollow"> [加為商友] </a><a rel="nofollow"> [發(fā)送信件] </a></p></div></div><div id="e3ruukv" class="page-proshow02"><p class="title">詳細說明</p><div id="3flhtek" class="box"><p><p style="text-indent:25px">8-羥基喹啉金屬配合物的制備與提純：對以8-羥基喹啉為配位體的金屬配合物合成過程中幾個重要的影響因素進行研究,發(fā)現(xiàn)反應溶液的濃度，泰州常見8-羥基喹啉、合成反應的時間、反應體系的pH值、反應溫度等因素對8-羥基喹啉金屬配合物的產率以及發(fā)光性能有很大的影響。結果表明:當8-羥基喹啉乙醇溶液濃度為80g/L,反應體系pH值為7.14,溫度為70℃,反應時間為3h時,Alq3的產率較高;反應體系pH值為10，泰州常見8-羥基喹啉,溫度為50℃，泰州常見8-羥基喹啉,反應時間為1h,Liq的產率較高;pH值為8,溫度為70℃,反應時間為1h,Znq2的產率較高。8-羥基喹啉基功能配合物在有機電致發(fā)光器件和有機太陽能電池領域具有比較良好的應用前景。泰州常見8-羥基喹啉</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="泰州常見8-羥基喹啉,8-羥基喹啉" src="https://tyunfile.71360.com/UploadFile/shbeicanghuagong/637326787858671875/6588095.png"></div><p style="text-indent:25px">鋁合金憑借優(yōu)良的機械性能、較小的相對密度、較好的kang沖擊性等特點得到了十分普遍的應用。但由于鋁合金性質活潑容易腐蝕而必須對其表面進行防腐處理。鉻酸鹽轉化膜技術是鋁及其合金表面處理比較常用的方法,但鉻酸鹽嚴重污染環(huán)境,在國際上已被明令禁止使用。所以,綠色環(huán)保的鋁合金表面無鉻轉化膜技術的研究與應用具有重要的現(xiàn)實意義。針對本課題組前期鋁合金表面制備氟鋁酸鹽轉化膜耐蝕性能還不夠理想的問題,本文對3003鋁合金表面氟鋁酸鹽轉化膜采用植酸、單寧酸、8-羥基喹啉三種有機物進行了耐蝕改性研究。泰州常見8-羥基喹啉8-羥基喹啉漏光會變成黑色，有石炭酸氣味。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="泰州常見8-羥基喹啉,8-羥基喹啉" src="https://tyunfile.71360.com/UploadFile/shbeicanghuagong/637326787878261718/4498780.png"></div><p style="text-indent:25px">5-氟-7-烯丙基-8-羥基喹啉的合成及生物活性測定：合成5-氟-7-烯丙基-8-羥基喹啉并測其農用生物活性。以4-氟苯酚為原料,經過醚化、Claisen重排,用發(fā)煙硝酸與乙酸酐硝化,用鋅粉還原硝基,然后與丙烯醛反應得到產物。產物的1HNMR及紅外分析與目標化合物一致;產物總收率為7.33%;產物對蘋果腐爛病菌、棉花枯萎病菌、柑橘炭疽病菌、小麥全蝕病菌的EC50值分別為36.78、68.36、34.51、94.73mg/L;質量濃度為100mg/L時,對稗草、反枝莧的胚根、胚軸的阻礙率均達到85%以上。以4-氟苯酚為原料進行醚化、重排、硝化還原、與丙烯醛反應來制備5-氟-7-烯丙基-8-羥基喹啉是一條可行的路線;產物具有良好的抑菌和除草活性。</p><p style="text-indent:25px">目前,制備8-羥基喹啉鋁常用的方法是在水和乙醇體系中,由8-羥基喹啉與鋁鹽在pH4。5~5。560~70度條件下反應約12h,或者在弱堿性條件下常溫反應約20h。用這些方法制備得到的8-羥基喹啉鋁往往是草綠色固體,純度一般在80%左右。為了滿足發(fā)光材料的純度要求,還需要通過柱色譜或升華方法提純,才能將8-羥基喹啉鋁的純度從80%左右提高到95%以上。制備8-羥基喹啉鋁一般在60~70度進行比較適合,為了得到高純度的8-羥基喹啉鋁,我們使用LC/MSD對在這一溫度下的8-羥基喹啉鋁的制備過程進行了跟蹤研究，發(fā)現(xiàn)體系的酸度和反應時間對產物純度及產率都有較大影響。8-羥基喹啉可用于測定鈷、鈾、鋁、鉬、鎘、釷、鐵、鈦、鎂、銅、鋅及有機氮的試劑。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="泰州常見8-羥基喹啉,8-羥基喹啉" src="https://tyunfile.71360.com/UploadFile/shbeicanghuagong/637326787936777343/947519.png"></div><p style="text-indent:25px">pH值分別對Cu-CQ，Pb-CQ，Cd-CQ和Zn-CQ絡合物（0.03 mol/L BR緩沖液）的峰值電流的影響。條件：Cu,Pb,Cd,Zn濃度10.0μg/L；CQ濃度：2.4 μmol/L；tads：30 s；Eads：－0.70V。在調制時間為40 ms時，得差分脈沖伏安圖，調制幅度：50mV；間隔時間：0.1s；電勢階躍：5 mV；掃描速率：50 mV/s。5-氯-7-碘-8羥基喹啉（CQ）吸附溶出伏安法同時測定痕量鉛、鎘和鋅的新方法。實驗用分離的銅、鉛、鎘和鋅溶液以及混合物進行，銅，鉛，鎘和鋅在（Britton Robinson緩沖液0.03mol/L）的zui佳pH值分別為2.3；5.1；5.3和5.2。除了zui佳的pH值，銅也不會干擾，但是無法同時測定四種元素，選擇pH5.3，CQ濃度3.6 μmol/ L和累積電勢－0.65V進行分析。銅、鉛、鎘和絡合物的峰值電流在－0.30；－0.41；－0.59和－0.95V，而自由CQ降低到－0.80V。分別分析，峰值電流與鉛，鎘和金屬濃度之間的線性關系分別直到40.0；31.0和70.0μɡ/L。8-羥基喹啉是化學分析的絡合滴定指示劑。泰州常見8-羥基喹啉</p><p style="text-indent:25px">恰當選擇8-羥基喹啉pH和掩蔽劑,可以改善試劑的選擇性。泰州常見8-羥基喹啉</p><p style="text-indent:25px">供試品中8-羥基喹啉出峰處有基質干擾？解決方案：1. 嘗試調整柱溫來改善分離，但無明顯效果。2. 對梯度條件進行優(yōu)化調整，甲醇初始比例由50%調整到40%；結果發(fā)現(xiàn)：供試品加標溶液中8-羥基喹啉與基質得到良好分離，同時對供試品及空白溶液進行分析，仍可得到良好結果。使用中等極性CAPCELL PAK C18 MGII S5; 4.6mm i.d.×250mm色譜柱，能夠得到8-羥基喹啉和硝羥喹啉的良好分析結果。由于不同樣品可能會帶來不同的基質干擾，需結合實際樣品對梯度條件進行調整。泰州常見8-羥基喹啉</p></p><br /><p>文章來源地址: http://www.cdcfah.com/cp/2503399.html</p></div></div></div></div></div><div id="nlh3coa" class="page-right twoColRt"><div id="ucd3pwl" class="box01 margin10 clearfix"><h3><a href="http://www.cdcfah.com/cp/">猜你喜歡</a></h3><div id="wpv3wwn" class="recomPic likePro"><a href="http://www.cdcfah.com/cp/814588.html"><div><img src="http://tyunfile.71360.com/UpLoadFile/2019/11/1/14/637082168864691056_lgpj_5374157.jpg" alt="福建ZF配件哪家強信息推薦自業(yè)物資供應" class="vcenter" onerror="javascript:this.src='/static/new_net_01/images/nopic.jpg';"></div><p>福建ZF配件哪家強信息推薦自業(yè)物資供應</p></a></div><div id="sbhtkw8" class="recomPic likePro"><a href="http://www.cdcfah.com/cp/846569.html"><div><img src="https://tyunfile.71360.com/WaterMark/UploadFile/nbzxsw/637298235378037109/764794.png" alt="寧波寧海直接考A2有幾個科目真誠推薦寧波助學商務信息咨詢供應" class="vcenter" 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