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onerror="javascript:this.src='/static/new_net_01/images/nopic.jpg';"></p></div></div></div><div id="vzvh8iz" class="content"><p><span>需求數(shù)量：</span>0</p><p><span>價(jià)格要求：</span>面議</p><p><span>所在地：</span>上海市</p><p><span>包裝要求：</span><span style="color: #f30;"></span></p><p><span>產(chǎn)品關(guān)鍵詞：</span>北京結(jié)構(gòu)確證怎么收費(fèi),結(jié)構(gòu)確證</p><p><span>***更新：</span>2021-01-13 04:08:32</p><p><span id="click" >瀏覽次數(shù)：0次</span></p><a rel="nofollow" class="button">聯(lián)系我們</a></div></div><div id="2pgx3nj" class="rightbox"><h3>公司基本資料信息</h3><p style="border:0;"><a rel="nofollow">上海微譜化工技術(shù)服務(wù)有限公司</a></p><p><span>聯(lián)系人：</span>趙佳林</p><p><span>郵箱: </span>506797994@qq.com</p><p><span>電話: </span>13916147713</p><p><span>傳真: </span>021_</p><p><span>網(wǎng)址: </span></p><p><span>手機(jī): </span>021-51045219</p><p><span>地址: </span>國(guó)偉路135號(hào)9號(hào)路</p><p>[當(dāng)前離線] <a rel="nofollow"> [加為商友] </a><a rel="nofollow"> [發(fā)送信件] </a></p></div></div><div id="b83yplm" class="page-proshow02"><p class="title">詳細(xì)說明</p><div id="jkqhagx" class="box"><p><p> 一般藥物的結(jié)構(gòu)確證方法有： </p> <p> 1.核磁共振:某些元素在分子中的類型、數(shù)目、相互連接方式、周圍化學(xué)環(huán)境、甚至空間排列等信息，進(jìn)而推測(cè)出化合物相應(yīng)官能團(tuán)的連接狀況及其初步的結(jié)構(gòu)。常用的有氫核磁共振譜(1H-NMR)和碳核磁共振譜( 13C-NMR)等。溶劑峰或部分溶劑中的溶劑化水峰可能會(huì)對(duì)部分信號(hào)有干擾作用，因此選擇適宜的溶劑或采用適宜的方法，以使所有信號(hào)得到充分顯示，對(duì)結(jié)構(gòu)解析有重要意義。 </p> <p> 微譜擁有完備的服務(wù)體系，可提供專業(yè)的實(shí)驗(yàn)室技術(shù)分析、檢測(cè)、研究開發(fā)、認(rèn)證、咨詢等服務(wù)，業(yè)務(wù)領(lǐng)域涵蓋材料化學(xué)，北京結(jié)構(gòu)確證怎么收費(fèi)、生物醫(yī)藥、生態(tài)環(huán)境、化妝品及日化品，北京結(jié)構(gòu)確證怎么收費(fèi)，北京結(jié)構(gòu)確證怎么收費(fèi)、食品、汽車等領(lǐng)域。 API結(jié)構(gòu)確證找哪家？找微譜！北京結(jié)構(gòu)確證怎么收費(fèi)</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="北京結(jié)構(gòu)確證怎么收費(fèi),結(jié)構(gòu)確證" src="https://tyunfile.71360.com/UploadFile/weipu02/637274715945908203/8091433.jpg"></div><p> 綜合解析：波譜數(shù)據(jù)、元素分析以及其它理化分析數(shù)據(jù)的綜合利用和解析，應(yīng)能**終確證該新藥的化學(xué)結(jié)構(gòu)（和構(gòu)型）。應(yīng)避免只羅列數(shù)據(jù)而無綜合解析，但也不需要過多的基本理論解說和繁復(fù)的推導(dǎo)，以簡(jiǎn)明扼要、合理充分為原則。綜合解析并無規(guī)定的統(tǒng)一格式和方法，大體上是按各種波譜和理化分析的各自特點(diǎn)，用所提供的信息解決分子結(jié)構(gòu)（和構(gòu)型）中某一個(gè)或某一部分問題。 </p> <p> 各種方法的總和和綜合解決有關(guān)分子結(jié)構(gòu)（和構(gòu)型）的全部問題。能夠清楚確證分子結(jié)構(gòu)（和構(gòu)型）而不存在疑問。中國(guó)臺(tái)灣結(jié)構(gòu)確證標(biāo)準(zhǔn)怎么做化藥結(jié)構(gòu)確證，找微譜！</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="北京結(jié)構(gòu)確證怎么收費(fèi),結(jié)構(gòu)確證" src="https://tyunfile.71360.com/UploadFile/weipu02/637274715949013672/6013798.jpg"></div><p> 復(fù)雜結(jié)構(gòu)化合物，當(dāng)一般的1H和13C譜不能對(duì)每個(gè)質(zhì)子和碳原子明確歸屬時(shí)，或圖譜峰過于擁擠，對(duì)解析結(jié)果有所疑問，應(yīng)考慮采用合適的其它技術(shù)確證，如1H譜中的各種去偶譜，H—Hcosy，以及局部圖形放大，13C譜中的Dept譜，以及H—C cosy。 </p> <p> 總之，務(wù)求對(duì)分子中全部H和C有合理和明確的解析。 </p> <p> 1H譜解析中所得數(shù)據(jù)應(yīng)按規(guī)定列表。對(duì)多重性明確的質(zhì)子，應(yīng)計(jì)算并列出相應(yīng)偶合常數(shù)J。13C譜解析數(shù)據(jù)也應(yīng)按歸定列表。Dept譜，H—H cosy譜，H-C cosy譜的解析和數(shù)據(jù)，除必要的文字說明外，也可列表，或在1H譜和13C譜數(shù)據(jù)表中增加相應(yīng)的欄目列出。 </p><p> 測(cè)試樣品必須是申報(bào)資料中所用生產(chǎn)工藝所得,按申報(bào)資料中精制方法精制。純度要求>99%，純度檢測(cè)按定方法。應(yīng)說明精制方法、樣品純度和純度檢測(cè)方法，附有關(guān)圖譜和數(shù)據(jù)。對(duì)照品指申報(bào)藥物為已知結(jié)構(gòu)藥物時(shí)，從有合法生產(chǎn)資格的非申報(bào)單位得到的符合法定標(biāo)準(zhǔn)的原料藥樣品應(yīng)提供對(duì)照品來源的合法證明、批號(hào)、提取精制方法、純度、純度檢測(cè)方法及相關(guān)圖譜。 </p> <p> <p> 微譜始終秉承“服務(wù)不止于檢測(cè)”的客戶服務(wù)理念，目前已與包括眾多世界500強(qiáng)企業(yè)在內(nèi)的近10萬家客戶建立了合作。 </p> 雜質(zhì)結(jié)構(gòu)確證，找微譜！</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="北京結(jié)構(gòu)確證怎么收費(fèi),結(jié)構(gòu)確證" src="https://tyunfile.71360.com/UploadFile/weipu02/637274715953359375/574181.jpg"></div><p style="text-indent:25px">如生物堿類的無機(jī)酸(如鹽酸、磷酸)鹽或簡(jiǎn)單有機(jī)酸(如酒石酸、枸櫞酸等)鹽，可采用成鹽前的游離堿基進(jìn)行波譜測(cè)定和解析,確證堿基結(jié)構(gòu)后，再經(jīng)確證成鹽情況，**終確證藥物結(jié)構(gòu)。如能同時(shí)提供成鹽前的堿(或酸)及鹽的兩套波譜和試驗(yàn)數(shù)據(jù)，是對(duì)結(jié)構(gòu)確證更充分和有力的證據(jù)。3.金屬鹽類和絡(luò)合物除通常要求的各項(xiàng)測(cè)試外，還應(yīng)提供確證分子中金屬元素存在和含量的有關(guān)圖譜和分析數(shù)據(jù)，以確證分子式。不適于或不能測(cè)試金屬鹽本身的項(xiàng)目，可以用成鹽前的酸分子或配位體相應(yīng)測(cè)試代替。結(jié)構(gòu)確證檢測(cè)，找微譜！北京結(jié)構(gòu)確證怎么收費(fèi)</p><p style="text-indent:25px">結(jié)構(gòu)確證找哪家？找微譜！北京結(jié)構(gòu)確證怎么收費(fèi)</p><p> 4.半合成化合物分子母核的結(jié)構(gòu)為已知并在合成過程中未發(fā)生改變的，可適當(dāng)簡(jiǎn)化對(duì)母核部分結(jié)構(gòu)的確證工作。重點(diǎn)在新的和發(fā)生改變的側(cè)鏈和取代的結(jié)構(gòu)確證，但必須提供證據(jù)證明原分子母核結(jié)構(gòu)在半合成全過程中未發(fā)生改變，可以結(jié)合原料結(jié)構(gòu)和合成路線進(jìn)行論證和說明。如涉及構(gòu)型確證，可以按上述同樣原則處理，即母核手性中心構(gòu)型沒有改變時(shí)，重點(diǎn)在于側(cè)鏈和職代基中新引入手性中心的構(gòu)型確定 </p> <p> 微譜具備國(guó)家認(rèn)可及授權(quán)的CMA、CNAS等資質(zhì)，被認(rèn)定為國(guó)家中小企業(yè)公共服務(wù)示范平臺(tái)、院士**工作站、****。北京結(jié)構(gòu)確證怎么收費(fèi)</p></p><br 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