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id="qvx4moi" class="proBig"><div id="2vsuw5k" class="bigimg"><div><p class="pic"><img src="https://tyunfile.71360.com/UploadFile/huixinghb/637254079271630860/5943745.jpg" class="vcenter" onerror="javascript:this.src='/static/new_net_01/images/nopic.jpg';"></p></div></div><div id="ixurtif" class="smallimg"><div><p class="pic"><img src="https://tyunfile.71360.com/UploadFile/huixinghb/637254079271630860/5943745.jpg" class="vcenter" onerror="javascript:this.src='/static/new_net_01/images/nopic.jpg';"></p></div></div></div><div id="dxh7wog" class="content"><p><span>需求數(shù)量：</span>0</p><p><span>價(jià)格要求：</span>面議</p><p><span>所在地：</span>廣東省</p><p><span>包裝要求：</span><span style="color: #f30;"></span></p><p><span>產(chǎn)品關(guān)鍵詞：</span>深圳塑料降解膜制造公司</p><p><span>***更新：</span>2020-05-31 10:19:57</p><p><span id="click" >瀏覽次數(shù)：3次</span></p><a rel="nofollow" class="button">聯(lián)系我們</a></div></div><div id="jtq2wvh" class="rightbox"><h3>公司基本資料信息</h3><p style="border:0;"><a rel="nofollow">廣東匯興環(huán)保材料有限公司</a></p><p><span>聯(lián)系人：</span>馮新科</p><p><span>郵箱: </span>sales@ti-bopp.com</p><p><span>電話(huà): </span>18807695431</p><p><span>傳真: </span>0769_</p><p><span>網(wǎng)址: </span></p><p><span>手機(jī): </span>0769-82275077</p><p><span>地址: </span>東坑鎮(zhèn)丁屋振興一路2號(hào)</p><p>[當(dāng)前離線(xiàn)] <a rel="nofollow"> [加為商友] </a><a rel="nofollow"> [發(fā)送信件] </a></p></div></div><div id="mgyacw7" class="page-proshow02"><p class="title">詳細(xì)說(shuō)明</p><div id="eikmoa2" class="box"><p><p style="text-indent:25px">本文對(duì)聚乳酸的合成方法及近年來(lái)聚乳酸基納米復(fù)合材料的研究進(jìn)展進(jìn)行了綜述,創(chuàng)新性地提出以L(fǎng)-乳酸和酸性硅溶膠(aSS)為原料的原位熔融縮聚法,制備了SiO_2含量為3.5％-19.1％的聚乳酸納米復(fù)合材料,并對(duì)聚乳酸/SiO_2納米復(fù)合材料的結(jié)構(gòu)、透光率、熱性能和結(jié)晶性進(jìn)行了較深入的研究。在L-乳酸熔融縮聚過(guò)程中,隨著聚乳酸分子量的提高,體系的極性發(fā)生明顯變化:由酸性單體的強(qiáng)極性/親水性變?yōu)榫廴樗岬娜鯓O性/親油性。本文選擇酸性硅溶膠(pH=2.5)與L-乳酸單體水溶液直接混合進(jìn)行原位分散。由于二者均為強(qiáng)酸性、強(qiáng)極性，深圳塑料降解膜制造公司，深圳塑料降解膜制造公司,且均為水分散液,確保了SiO_2粒子的分散穩(wěn)定,且方便地實(shí)現(xiàn)了SiO_2粒子在L-乳酸單體中的均勻分散。在縮聚過(guò)程中,一方面有機(jī)相由于聚乳酸鏈的增長(zhǎng),使極性變?nèi)?而無(wú)機(jī)相SiO_2粒子表面分布有活性高的硅羥基,可以與L-乳酸單體(LLA)和乳酸齊聚物(OLLA)的羧基發(fā)生縮合反應(yīng)，深圳塑料降解膜制造公司,使OLLA接枝到SiO_2表面,隨著接枝反應(yīng)的進(jìn)行以及g-OLLA鏈的增長(zhǎng),無(wú)機(jī)相的極性也逐漸減弱,因而無(wú)機(jī)相表面也發(fā)生與有機(jī)相同步的極性變化；</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="深圳塑料降解膜制造公司" src="https://tyunfile.71360.com/UploadFile/huixinghb/637254079271630860/5943745.jpg"></div><p> <br /> </p> <p> 采用原位聚合的方法制備了有機(jī)化處理過(guò)的納米TiO2粒子質(zhì)量分?jǐn)?shù)分別為1 wt%、3 wt%、5 wt%和10 wt%的4種納米TiO2/聚乳酸復(fù)合材料。SEM結(jié)果表明,當(dāng)納米TiO2粒子質(zhì)量分?jǐn)?shù)較低時(shí),納米TiO2在聚乳酸基體中呈現(xiàn)均勻穩(wěn)定分散,而質(zhì)量分?jǐn)?shù)較高時(shí)則發(fā)生團(tuán)聚。通過(guò)力學(xué)和熱學(xué)等性能測(cè)試發(fā)現(xiàn)復(fù)合材料的比較大熱分解溫度、玻璃化轉(zhuǎn)變溫度和力學(xué)性能相對(duì)于聚乳酸有較大幅度提高,其中納米TiO2的質(zhì)量分?jǐn)?shù)為3 wt%時(shí)改善效果**明顯,其比較大熱分解溫度、玻璃化轉(zhuǎn)變溫度分別比聚乳酸提高了25.3℃和4.9℃,拉伸強(qiáng)度、斷裂伸長(zhǎng)率和彈性模量分別提高了83.6%、6.73%和129.4%。 </p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="深圳塑料降解膜制造公司" src="https://tyunfile.71360.com/UploadFile/huixinghb/637254079271142578/7390182.jpg"></div><p style="text-indent:25px">熔融縮聚法,制備了SiO_2含量為3.5％-19.1％的聚乳酸納米復(fù)合材料,并對(duì)聚乳酸/SiO_2納米復(fù)合材料的結(jié)構(gòu)、透光率、熱性能和結(jié)晶性進(jìn)行了較深入的研究。在L-乳酸熔融縮聚過(guò)程中,隨著聚乳酸分子量的提高,體系的極性發(fā)生明顯變化:由酸性單體的強(qiáng)極性/親水性變?yōu)榫廴樗岬娜鯓O性/親油性。本文選擇酸性硅溶膠(pH=2.5)與L-乳酸單體水溶液直接混合進(jìn)行原位分散。由于二者均為強(qiáng)酸性、強(qiáng)極性,且均為水分散液,確保了SiO_2粒子的分散穩(wěn)定,且方便地實(shí)現(xiàn)了SiO_2粒子在L-乳酸單體中的均勻分散。在縮聚過(guò)程中,一方面有機(jī)相由于聚乳酸鏈的增長(zhǎng),使極性變?nèi)?而無(wú)機(jī)相SiO_2粒子表面分布有活性高的硅羥基,可以與L-乳酸單體(LLA)和乳酸齊聚物(OLLA)的羧基發(fā)生縮合反應(yīng),使OLLA接枝到SiO_2表面,隨著接枝反應(yīng)的進(jìn)行以及g-OLLA鏈的增長(zhǎng),無(wú)機(jī)相的極性也逐漸減弱,因而無(wú)機(jī)相表面也發(fā)生與有機(jī)相同步的極性變化；另一方面,g-OLLA在SiO_2粒子表面取代擴(kuò)散雙電層形成保護(hù)層,提供了位阻效應(yīng)。二者均起到了促進(jìn)SiO_2粒子分散穩(wěn)定的作用,因此**終能得到SiO_2粒子在聚乳酸基體中納米級(jí)分散的聚乳酸/SiO_2納米復(fù)合材料。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="深圳塑料降解膜制造公司" src="https://tyunfile.71360.com/UploadFile/huixinghb/637254079237246094/5981543.jpg"></div></p><br /><p>文章來(lái)源地址: 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