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onerror="javascript:this.src='/static/new_net_01/images/nopic.jpg';"></p></div></div><div id="mgxj7qs" class="smallimg"><div><p class="pic"><img src="https://tyunfile.71360.com/WaterMark/UploadFile//637280289509208985/415071.png" class="vcenter" onerror="javascript:this.src='/static/new_net_01/images/nopic.jpg';"></p></div></div></div><div id="ful2zdn" class="content"><p><span>需求數(shù)量：</span>0</p><p><span>價格要求：</span>面議</p><p><span>所在地：</span>上海市</p><p><span>包裝要求：</span><span style="color: #f30;"></span></p><p><span>產(chǎn)品關(guān)鍵詞：</span>***泛解酸內(nèi)酯中間體</p><p><span>***更新：</span>2020-06-22 00:39:30</p><p><span id="click" >瀏覽次數(shù)：0次</span></p><a rel="nofollow" class="button">聯(lián)系我們</a></div></div><div id="yifbs8d" class="rightbox"><h3>公司基本資料信息</h3><p style="border:0;"><a rel="nofollow">上海臨辰醫(yī)藥科技有限公司</a></p><p><span>聯(lián)系人：</span>葉海岑</p><p><span>郵箱: </span>info@linchenpharm.com</p><p><span>電話: </span>13761181955</p><p><span>傳真: </span>021_</p><p><span>網(wǎng)址: </span></p><p><span>手機: </span>021-31606595</p><p><span>地址: </span>辰花路5088弄221號</p><p>[當(dāng)前離線] <a rel="nofollow"> [加為商友] </a><a rel="nofollow"> [發(fā)送信件] </a></p></div></div><div id="fu8jsle" class="page-proshow02"><p class="title">詳細說明</p><div id="2qkryu5" class="box"><p><p> 在產(chǎn)能分布上，國內(nèi)鑫富藥業(yè)產(chǎn)能比較大，約為7,000噸。2011年日本地震后，由于基礎(chǔ)設(shè)施被破壞，日本精化暫停了泛酸鈣的生產(chǎn)。在該品種上，精化盈利情況并不理想，地震破壞了生產(chǎn)所需的基礎(chǔ)設(shè)施，***泛解酸內(nèi)酯中間體，影響較為嚴重，未來有可能退出泛酸鈣市場。 </p> <p> 泛解酸內(nèi)酯中的D 構(gòu)型，將水解產(chǎn)物D 泛解酸分離出來，***泛解酸內(nèi)酯中間體，***泛解酸內(nèi)酯中間體，再經(jīng)過內(nèi)酯化轉(zhuǎn)變成D 泛解酸內(nèi)酯，此方法已由日本制藥（FUJI）公司申請了專利，并投入工業(yè)化生產(chǎn)。 </p> <p> 海藻酸鈉及其與聚丙烯酰胺(PAM)和聚乙烯醇(PVA)的復(fù)合載體對鐮孢霉菌(Fusarium oxysporum BU-11)細胞的固定，該固定化細胞被用于手性拆分D,L-泛解酸內(nèi)酯的反應(yīng)體系。 </p> <p> <br /> </p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="***泛解酸內(nèi)酯中間體" src="https://tyunfile.71360.com/WaterMark/UploadFile//637280289509208985/415071.png"></div><p style="text-indent:25px">一種ＤＬ－泛酰內(nèi)酯的拆分方法?，F(xiàn)有拆分方法中使用的拆分劑在拆分ＤＬ－泛酰內(nèi)酯時的選擇性低，使ＤＬ－泛酰內(nèi)酯的總利用率低，提高了拆分ＤＬ－泛酰內(nèi)酯的生產(chǎn)成本。本發(fā)明所用的拆分劑為有機堿Ｒ－ＮＨ＃－［２］，其中Ｒ為Ｃ＃－［１５］Ｈ＃－［１５］，包括以下步驟：ａ）用純化后的拆分劑與酸反應(yīng)，加水、加熱溶解，滴加ＤＬ－泛酰內(nèi)酯水解液，拆分劑：ＤＬ－泛酰內(nèi)酯的摩爾比＝０．５－０．７∶１；ｂ）抽濾由ａ得到的反應(yīng)液，濾餅進行消旋、回收拆分劑處理，濾液加入有機溶劑進行共沸脫水，蒸去過量有機溶劑進行結(jié)晶。本發(fā)明明顯提高了拆分劑對Ｄ－泛酰內(nèi)酯的選擇性，提高ＤＬ－泛酰內(nèi)酯的總利用率，拆分收率高，減少拆分劑的用量且容易重復(fù)回收利用，降低拆分ＤＬ－泛酰內(nèi)酯的生產(chǎn)成本。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="***泛解酸內(nèi)酯中間體" src="https://tyunfile.71360.com/WaterMark/UploadFile//637280289746210938/9268872.png"></div><p style="text-indent:25px">D-泛解酸內(nèi)酯?，F(xiàn)有技術(shù)中還有在培養(yǎng)基中培養(yǎng)尖孢鐮孢菌，在培養(yǎng)后的尖孢鐮孢菌與底物混合，水解得到D-泛解酸，內(nèi)酯化獲得D-泛解酸內(nèi)酯，但是本方法采用發(fā)酵制備D-泛解酸內(nèi)酯的過程能耗較高，且產(chǎn)率低，工業(yè)成本較高?，F(xiàn)有技術(shù)中還有以水和甲苯為溶劑體系，通過添加D-泛解酸內(nèi)酯作為晶種，誘導(dǎo)結(jié)晶獲得D-泛解酸內(nèi)酯的方法，但是本方法在生產(chǎn)過程中采用了甲苯，生產(chǎn)過程VOC排放較高，且通過誘導(dǎo)結(jié)晶獲得的一次收率較低，產(chǎn)品比旋度較低。</p></p><br /><p>文章來源地址: http://www.cdcfah.com/cp/343799.html</p></div></div></div></div></div><div id="pnpbsed" class="page-right twoColRt"><div id="88oac7h" class="box01 margin10 clearfix"><h3><a href="http://www.cdcfah.com/cp/">猜你喜歡</a></h3><div id="ih8xlcq" class="recomPic likePro"><a href="http://www.cdcfah.com/cp/814588.html"><div><img src="http://tyunfile.71360.com/UpLoadFile/2019/11/1/14/637082168864691056_lgpj_5374157.jpg" alt="福建ZF配件哪家強信息推薦自業(yè)物資供應(yīng)" class="vcenter" onerror="javascript:this.src='/static/new_net_01/images/nopic.jpg';"></div><p>福建ZF配件哪家強信息推薦自業(yè)物資供應(yīng)</p></a></div><div id="kelselx" 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