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class="bigimg"><div><p class="pic"><img src="https://tyunfile.71360.com/WaterMark/UploadFile/shlinchen/637278339844755859/788254.png" class="vcenter" onerror="javascript:this.src='/static/new_net_01/images/nopic.jpg';"></p></div></div><div id="3729zbd" class="smallimg"><div><p class="pic"><img src="https://tyunfile.71360.com/WaterMark/UploadFile/shlinchen/637278339844755859/788254.png" class="vcenter" onerror="javascript:this.src='/static/new_net_01/images/nopic.jpg';"></p></div></div></div><div id="5vwb87f" class="content"><p><span>需求數(shù)量：</span>0</p><p><span>價(jià)格要求：</span>面議</p><p><span>所在地：</span>上海市</p><p><span>包裝要求：</span><span style="color: #f30;"></span></p><p><span>產(chǎn)品關(guān)鍵詞：</span>品質(zhì)泛解酸內(nèi)酯批發(fā)價(jià)</p><p><span>***更新：</span>2020-06-24 10:28:27</p><p><span id="click" >瀏覽次數(shù)：0次</span></p><a rel="nofollow" class="button">聯(lián)系我們</a></div></div><div id="fug8h8p" class="rightbox"><h3>公司基本資料信息</h3><p style="border:0;"><a rel="nofollow">上海臨辰醫(yī)藥科技有限公司</a></p><p><span>聯(lián)系人：</span>葉海岑</p><p><span>郵箱: </span>info@linchenpharm.com</p><p><span>電話: </span>13761181955</p><p><span>傳真: </span>021_</p><p><span>網(wǎng)址: </span></p><p><span>手機(jī): </span>021-31606595</p><p><span>地址: </span>辰花路5088弄221號(hào)</p><p>[當(dāng)前離線] <a rel="nofollow"> [加為商友] </a><a rel="nofollow"> [發(fā)送信件] </a></p></div></div><div id="c74y24y" class="page-proshow02"><p class="title">詳細(xì)說(shuō)明</p><div id="rbixdrd" class="box"><p><p> 化還原酶催化不對(duì)稱還原制備D-泛解酸內(nèi)酯氧化還原酶不對(duì)稱還原酮泛解酸內(nèi)酯的方法。用L-泛解酸內(nèi)酯脫氫酶將L-泛解酸內(nèi)酯氧化成酮泛解酸內(nèi)酯，再利用酮泛解酸內(nèi)酯還原酶將其不對(duì)稱還原成D-泛解酸內(nèi)酯。該方法也可將外消旋的泛解酸內(nèi)酯作為起始原料，經(jīng)過(guò)氧化還原反應(yīng)后得到D-泛解酸內(nèi)酯，品質(zhì)泛解酸內(nèi)酯批發(fā)價(jià)，過(guò)程簡(jiǎn)單，品質(zhì)泛解酸內(nèi)酯批發(fā)價(jià)，不需要化學(xué)法中的再消旋化反應(yīng)。 </p> <p> <p> 制備方法包括以下步驟：(1)將纈氨酸在過(guò)氧化氫酶和α?酮異戊酸還原酶的作用下，品質(zhì)泛解酸內(nèi)酯批發(fā)價(jià)，進(jìn)行酶轉(zhuǎn)化得到α?酮異戊酸； </p> <p> <br /> </p> <p> (2)將所述α?酮異戊酸與四氫葉酸在羥甲基轉(zhuǎn)移酶和氯化鎂的作用下，反應(yīng)制備酮泛解酸； </p> <p> <br /> </p> <p> (3)將所述酮泛解酸在α?酮異戊酸還原酶的作用下，進(jìn)行酶轉(zhuǎn)化得到泛解酸； </p> <p> <br /> </p> <p> (4)將所述泛解酸制備得到泛解酸內(nèi)酯。 </p> </p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="品質(zhì)泛解酸內(nèi)酯批發(fā)價(jià)" src="https://tyunfile.71360.com/WaterMark/UploadFile/shlinchen/637278339844755859/788254.png"></div><p> ＤＬ－泛酰內(nèi)酯的拆分方法，所用的拆分劑為有機(jī)堿Ｒ－ＮＨ↓［２］，其中Ｒ為Ｃ↓［１５］Ｈ↓［１５］，包括以下步驟：ａ）用純化后的拆分劑與酸反應(yīng)，生成物加水，加熱至８０－８５℃溶解，在攪拌下滴加ＤＬ－泛酰內(nèi)酯水解液，拆分劑：ＤＬ－泛酰內(nèi)酯的摩爾比＝０．５－０．７∶１，反應(yīng)溫度控制在４５－５５℃，滴加完畢后繼續(xù)攪拌０．５－１．５小時(shí)，然后在室溫下自然冷卻至２０－３０℃；ｂ）真空抽濾由ａ得到的反應(yīng)液，濾餅進(jìn)行消旋、回收拆分劑處理，濾液減壓蒸餾去水，然后加入有機(jī)溶劑進(jìn)行共沸脫水，殘留水分脫去后，蒸去過(guò)量有機(jī)溶劑進(jìn)行冷卻結(jié)晶，過(guò)濾得Ｌ－泛酰內(nèi)酯。 </p> <p> <br /> </p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="品質(zhì)泛解酸內(nèi)酯批發(fā)價(jià)" src="https://tyunfile.71360.com/WaterMark/UploadFile/shlinchen/637278336133632812/8293857.png"></div><p> 在產(chǎn)能分布上，國(guó)內(nèi)鑫富藥業(yè)產(chǎn)能比較大，約為7,000噸。2011年日本地震后，由于基礎(chǔ)設(shè)施被破壞，日本精化暫停了泛酸鈣的生產(chǎn)。在該品種上，精化盈利情況并不理想，地震破壞了生產(chǎn)所需的基礎(chǔ)設(shè)施，影響較為嚴(yán)重，未來(lái)有可能退出泛酸鈣市場(chǎng)。 </p> <p> 泛解酸內(nèi)酯中的D 構(gòu)型，將水解產(chǎn)物D 泛解酸分離出來(lái)，再經(jīng)過(guò)內(nèi)酯化轉(zhuǎn)變成D 泛解酸內(nèi)酯，此方法已由日本制藥（FUJI）公司申請(qǐng)了專利，并投入工業(yè)化生產(chǎn)。 </p> <p> 海藻酸鈉及其與聚丙烯酰胺(PAM)和聚乙烯醇(PVA)的復(fù)合載體對(duì)鐮孢霉菌(Fusarium oxysporum BU-11)細(xì)胞的固定，該固定化細(xì)胞被用于手性拆分D,L-泛解酸內(nèi)酯的反應(yīng)體系。 </p> <p> <br /> </p></p><br /><p>文章來(lái)源地址: http://www.cdcfah.com/cp/373425.html</p></div></div></div></div></div><div id="q84maev" class="page-right twoColRt"><div id="gq34p22" class="box01 margin10 clearfix"><h3><a href="http://www.cdcfah.com/cp/">猜你喜歡</a></h3><div id="727tfjv" class="recomPic likePro"><a href="http://www.cdcfah.com/cp/814588.html"><div><img 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