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class="pic"><img src="https://tyunfile.71360.com/WaterMark/UploadFile//637280289746210938/9268872.png" class="vcenter" onerror="javascript:this.src='/static/new_net_01/images/nopic.jpg';"></p></div></div><div id="c89eb84" class="smallimg"><div><p class="pic"><img src="https://tyunfile.71360.com/WaterMark/UploadFile//637280289746210938/9268872.png" class="vcenter" onerror="javascript:this.src='/static/new_net_01/images/nopic.jpg';"></p></div></div></div><div id="9z4nprl" class="content"><p><span>需求數(shù)量：</span>0</p><p><span>價(jià)格要求：</span>面議</p><p><span>所在地：</span>上海市</p><p><span>包裝要求：</span><span style="color: #f30;"></span></p><p><span>產(chǎn)品關(guān)鍵詞：</span>99泛解酸內(nèi)酯企業(yè)</p><p><span>***更新：</span>2020-06-25 14:54:45</p><p><span id="click" >瀏覽次數(shù)：0次</span></p><a rel="nofollow" class="button">聯(lián)系我們</a></div></div><div id="the3hg8" class="rightbox"><h3>公司基本資料信息</h3><p style="border:0;"><a rel="nofollow">上海臨辰醫(yī)藥科技有限公司</a></p><p><span>聯(lián)系人：</span>葉海岑</p><p><span>郵箱: </span>info@linchenpharm.com</p><p><span>電話(huà): </span>13761181955</p><p><span>傳真: </span>021_</p><p><span>網(wǎng)址: </span></p><p><span>手機(jī): </span>021-31606595</p><p><span>地址: </span>辰花路5088弄221號(hào)</p><p>[當(dāng)前離線(xiàn)] <a rel="nofollow"> [加為商友] </a><a rel="nofollow"> [發(fā)送信件] </a></p></div></div><div id="hyfczwl" class="page-proshow02"><p class="title">詳細(xì)說(shuō)明</p><div id="3po7z8p" class="box"><p><p style="text-indent:25px">一種高純度的D?泛酸內(nèi)酯的合成方法包括步驟:將DL?泛酸內(nèi)酯加入到水中,在pH為6.0?8.0用酶水解,得到D?泛解酸以及L?泛酸內(nèi)酯;將上述水溶液經(jīng)有機(jī)溶劑萃取,得到D?泛解酸的水溶液以及L?泛酸內(nèi)酯有機(jī)溶液;將D?泛解酸的水溶液,控溫20?80℃反應(yīng),用酸調(diào)節(jié)pH至1?4,然后關(guān)環(huán)得到D?泛酸內(nèi)酯水溶液;將步驟S3所得的D?泛酸內(nèi)酯水溶液經(jīng)有機(jī)溶劑萃取,然后經(jīng)濃縮,蒸餾,結(jié)晶得到D?泛酸內(nèi)酯;將步驟S2所得的L?泛酸內(nèi)酯溶液經(jīng)濃縮、然后在堿性條件下消旋得到DL?泛酸內(nèi)酯。本發(fā)明為泛酸鈣制備得到D?泛酸內(nèi)酯，99泛解酸內(nèi)酯企業(yè),工藝路線(xiàn)操作簡(jiǎn)單,反應(yīng)條件溫和,安全，99泛解酸內(nèi)酯企業(yè),環(huán)保，99泛解酸內(nèi)酯企業(yè),原料價(jià)廉易得,工業(yè)適應(yīng)性強(qiáng)。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="99泛解酸內(nèi)酯企業(yè)" src="https://tyunfile.71360.com/WaterMark/UploadFile//637280289746210938/9268872.png"></div><p style="text-indent:25px">一種ＤＬ－泛酰內(nèi)酯的拆分方法?，F(xiàn)有拆分方法中使用的拆分劑在拆分ＤＬ－泛酰內(nèi)酯時(shí)的選擇性低，使ＤＬ－泛酰內(nèi)酯的總利用率低，提高了拆分ＤＬ－泛酰內(nèi)酯的生產(chǎn)成本。本發(fā)明所用的拆分劑為有機(jī)堿Ｒ－ＮＨ＃－［２］，其中Ｒ為Ｃ＃－［１５］Ｈ＃－［１５］，包括以下步驟：ａ）用純化后的拆分劑與酸反應(yīng)，加水、加熱溶解，滴加ＤＬ－泛酰內(nèi)酯水解液，拆分劑：ＤＬ－泛酰內(nèi)酯的摩爾比＝０．５－０．７∶１；ｂ）抽濾由ａ得到的反應(yīng)液，濾餅進(jìn)行消旋、回收拆分劑處理，濾液加入有機(jī)溶劑進(jìn)行共沸脫水，蒸去過(guò)量有機(jī)溶劑進(jìn)行結(jié)晶。本發(fā)明明顯提高了拆分劑對(duì)Ｄ－泛酰內(nèi)酯的選擇性，提高ＤＬ－泛酰內(nèi)酯的總利用率，拆分收率高，減少拆分劑的用量且容易重復(fù)回收利用，降低拆分ＤＬ－泛酰內(nèi)酯的生產(chǎn)成本。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="99泛解酸內(nèi)酯企業(yè)" src="https://tyunfile.71360.com/WaterMark/UploadFile//637280289625869141/3735503.png"></div><p> D-泛酸鈣的制備方法主要有兩種：1)先化學(xué)合成DL-泛酸鈣，通過(guò)拆分DL-泛酸鈣而制得D-泛酸鈣。2)通過(guò)化學(xué)法或生物法拆分關(guān)鍵中間體DL-泛解酸內(nèi)酯得到D-泛解酸內(nèi)酯，再由D-泛解酸內(nèi)酯與β--氨基丙酸反應(yīng)合成D-泛酸鈣，其中生物法拆分的成本比化學(xué)法拆分的成本低15%。 </p> <p> 國(guó)外D-泛酸鈣生產(chǎn)公司主要有日本制藥精細(xì)化學(xué)品公司、德國(guó)BASF公司、荷蘭DSM公司等。BASF、DSM均采用化學(xué)法生產(chǎn)，而日本***制藥采用生物法酶拆分工藝制備中間體D-泛解酸內(nèi)酯，這也是目前**技術(shù)的工藝。國(guó)內(nèi)原只有鑫富藥業(yè)一家有生物法酶拆分工藝，但現(xiàn)在山東新發(fā)也采用了這一工藝。 </p> <p> <br /> </p></p><br /><p>文章來(lái)源地址: http://www.cdcfah.com/cp/387864.html</p></div></div></div></div></div><div id="zh3rt3j" class="page-right twoColRt"><div id="i7jjg8i" class="box01 margin10 clearfix"><h3><a href="http://www.cdcfah.com/cp/">猜你喜歡</a></h3><div id="vdahoah" class="recomPic likePro"><a href="http://www.cdcfah.com/cp/814588.html"><div><img src="http://tyunfile.71360.com/UpLoadFile/2019/11/1/14/637082168864691056_lgpj_5374157.jpg" alt="福建ZF配件哪家強(qiáng) 信息推薦自業(yè)物資供應(yīng)" class="vcenter" onerror="javascript:this.src='/static/new_net_01/images/nopic.jpg';"></div><p>福建ZF配件哪家強(qiáng) 信息推薦自業(yè)物資供應(yīng)</p></a></div><div id="dbnkm8t" class="recomPic likePro"><a href="http://www.cdcfah.com/cp/846569.html"><div><img 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