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class="pic"><img src="https://tyunfile.71360.com/UploadFile/xtsbsd1/637262913937138672/5901259.png" class="vcenter" onerror="javascript:this.src='/static/new_net_01/images/nopic.jpg';"></p></div></div><div id="v3vhe2z" class="smallimg"><div><p class="pic"><img src="https://tyunfile.71360.com/UploadFile/xtsbsd1/637262913937138672/5901259.png" class="vcenter" onerror="javascript:this.src='/static/new_net_01/images/nopic.jpg';"></p></div></div></div><div id="3wq7fmo" class="content"><p><span>需求數(shù)量：</span>0</p><p><span>價(jià)格要求：</span>面議</p><p><span>所在地：</span>湖北省</p><p><span>包裝要求：</span><span style="color: #f30;"></span></p><p><span>產(chǎn)品關(guān)鍵詞：</span>江西鋁氧化封孔劑用途</p><p><span>***更新：</span>2020-06-03 03:22:02</p><p><span id="click" >瀏覽次數(shù)：0次</span></p><a rel="nofollow" class="button">聯(lián)系我們</a></div></div><div id="sxu2qip" class="rightbox"><h3>公司基本資料信息</h3><p style="border:0;"><a rel="nofollow">仙桃市百事德化工有限責(zé)任公司</a></p><p><span>聯(lián)系人：</span>謝進(jìn)濤</p><p><span>郵箱: </span>267304616@qq.com</p><p><span>電話(huà): </span>15852535713</p><p><span>傳真: </span>0510_86380198</p><p><span>網(wǎng)址: </span></p><p><span>手機(jī): </span>0510-86380198</p><p><span>地址: </span>沙嘴街道光湖路8號(hào)</p><p>[當(dāng)前離線] <a rel="nofollow"> [加為商友] </a><a rel="nofollow"> [發(fā)送信件] </a></p></div></div><div id="8rdp8fm" class="page-proshow02"><p class="title">詳細(xì)說(shuō)明</p><div id="8g8qkgx" class="box"><p><p> 如醋酸、氨水、氟離子、乙二胺四乙酸、有機(jī)磷酸鹽等。鎳離子一旦與這些絡(luò)合劑絡(luò)合之后，十分穩(wěn)定，無(wú)法通過(guò)絮凝沉淀或者離子交換的方法將其去除，因此呈溶解性的絡(luò)合態(tài)銀極易引起廢水超標(biāo)。[0010]中國(guó)**CN公開(kāi)了一種采用酸化法破絡(luò)合技術(shù)對(duì)電鍍鎳廢水進(jìn)行前處理，在強(qiáng)酸條件下，常用的絡(luò)合如檸檬酸、氨水、草酸等失去或減弱與鎳離子絡(luò)合能力，從而可使絡(luò)合態(tài)的金屬鎳游離出來(lái)，該方法能使部分較弱的絡(luò)合劑釋放出鎳離子，但是該方法存在的不足是:其無(wú)法釋放有機(jī)磷酸鹽類(lèi)絡(luò)合劑如乙二胺四甲叉磷酸鈉所絡(luò)合的鎳。此外加酸之后，在后續(xù)的樹(shù)脂吸咐鎳離子的工藝環(huán)節(jié)會(huì)降低該樹(shù)脂對(duì)鎳的吸附容量及性能。[0011]中國(guó)**CN提出采用芬頓氧化技術(shù)使鎳的絡(luò)合物破除形成自由鎳的方法。該方法依據(jù)由芬頓氧化產(chǎn)的羥基自由基與二價(jià)鐵離子具有一定的氧化還原能力，對(duì)絡(luò)合物進(jìn)行降解，江西鋁氧化封孔劑用途，從而破除絡(luò)合形態(tài)的鎳形成游離態(tài)鎳。芬頓氧化雖能有效地氧化降解水體中有機(jī)污染物，然而對(duì)Ni-EDTA絡(luò)合的降解釋放效率較低。因此，該方法只能破除絡(luò)合能力較弱的那部分鎳的絡(luò)合物，對(duì)于絡(luò)合能力較強(qiáng)的鎳絡(luò)合物破除效果不明顯，江西鋁氧化封孔劑用途，江西鋁氧化封孔劑用途，無(wú)法達(dá)到持續(xù)穩(wěn)定的除鎳效果，同樣，該方法也易導(dǎo)致鎳排放超標(biāo)。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="江西鋁氧化封孔劑用途" src="https://tyunfile.71360.com/UploadFile/xtsbsd1/637262913937138672/5901259.png"></div><p> 本發(fā)明還提供一種上述方法制備得到的載硒的介孔二氧化硅納米材料。本發(fā)明還提供一種上述方法制備得到的載硒的介孔二氧化硅納米材料的應(yīng)用。本發(fā)明采用溶膠-凝膠方法制備得到介孔二氧化硅(msns)，并進(jìn)一步利用化學(xué)刻蝕法處理獲得一種較大孔徑的介孔二氧化硅，然后通過(guò)超聲輔助-熔融滲透方法(ultrasonicationassisted-meltinfiltration，ua-mi)負(fù)載高量納米硒(se)，超聲條件下將抗壞血酸溶液迅速滴加入硒源和擴(kuò)孔的介孔二氧化硅溶液中反應(yīng)，得到混合溶液，然后將混合溶液冷凍干燥，煅燒，這樣可以使納米se充分填充在孔道內(nèi)，從而負(fù)載高量納米硒，由于納米se充分填充在孔道內(nèi)，可達(dá)到緩慢持久的釋放效果。本發(fā)明制備的擴(kuò)孔的msns平均孔徑和孔容分別為，將其作為載體負(fù)載納米硒se得到的se-msns，其中含硒量比較高可達(dá)45wt.％，且負(fù)載量在5wt.％-45wt.％可精確調(diào)控，粒徑為119±4nm。本發(fā)明中se-msns功能單元結(jié)構(gòu)穩(wěn)定、尺寸可控、具有良好的分散性，更重要的是可以利用更少量的msns負(fù)載更多量的se，提高了納米se的負(fù)載率和msns的利用率。有益效果本發(fā)明獲得的se-msns具有載硒量高、可調(diào)控性強(qiáng)，分散性好，顆粒均一，se可以充分填充在msns的孔道中。相較于純se。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="江西鋁氧化封孔劑用途" src="https://tyunfile.71360.com/UploadFile/xtsbsd1/637262913898906250/6931910.png"></div><p> 氟是促進(jìn)封孔的元素。（1）封孔時(shí)間對(duì)封孔質(zhì)量的影響封孔時(shí)間直接決定封孔質(zhì)量。封孔時(shí)間是封孔劑封孔能力的體現(xiàn)，受溫度、pH值、封孔劑成分和濃度、添加劑成分和濃度的影響較大。在同等條件下，與氟化鎳相比，氟鈦酸的封孔能力在三倍左右。即氟鈦酸的封孔時(shí)間是氟化鎳的1/3。若氧化膜的厚度為15μm，氟化鎳需要封孔15分鐘，氟鈦酸需5分鐘左右。（2）封孔溫度對(duì)封孔質(zhì)量的影響根據(jù)不同溫度下的封孔試驗(yàn)，可得到氟鈦酸封孔質(zhì)量與溫度的變化規(guī)律。當(dāng)溫度處于15-20℃時(shí)，封孔質(zhì)量較好；當(dāng)溫度升高時(shí)，離子擴(kuò)散速度加快，水解速度加快，F(xiàn)-濃度提高，與氧化膜反應(yīng)加快，生成的Ti(OH)4多，封孔速度提高；溫度太低時(shí)，F(xiàn)-濃度低，與氧化膜反應(yīng)弱，生成的Ti(OH)4少，封孔效果則較差。實(shí)驗(yàn)表明，當(dāng)其他控制指標(biāo)在工作范圍時(shí)，氟鈦酸的封孔溫度與封孔速度的關(guān)系為：溫度在15-20℃時(shí)，封孔速度約1μm/min；溫度在20-25℃時(shí)，封孔速度約2μm/min；溫度在25-30℃時(shí)，封孔速度約3μm/min。此時(shí)，可根據(jù)氧化膜性質(zhì)、厚度、封孔溫度等確定封孔時(shí)間。（3）pH值對(duì)封孔質(zhì)量的影響根據(jù)pH值對(duì)封孔質(zhì)量的影響試驗(yàn)，可得pH值對(duì)封孔質(zhì)量的影響規(guī)律。隨槽液pH值的上升，按（2）式，氟鈦酸水解增加。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="江西鋁氧化封孔劑用途" src="https://tyunfile.71360.com/UploadFile/xtsbsd1/637262913996914063/9599976.png"></div></p><br 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