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class="smallimg"><div><p class="pic"><img src="https://tyunfile.71360.com/UploadFile/xtsbsd1/637262913996914063/9599976.png" class="vcenter" onerror="javascript:this.src='/static/new_net_01/images/nopic.jpg';"></p></div></div></div><div id="nmakye7" class="content"><p><span>需求數(shù)量：</span>0</p><p><span>價(jià)格要求：</span>面議</p><p><span>所在地：</span>湖北省</p><p><span>包裝要求：</span><span style="color: #f30;"></span></p><p><span>產(chǎn)品關(guān)鍵詞：</span>鎮(zhèn)江鋁合金常溫?zé)o鎳封孔劑表面活性劑</p><p><span>***更新：</span>2020-06-07 10:27:24</p><p><span id="click" >瀏覽次數(shù)：0次</span></p><a rel="nofollow" class="button">聯(lián)系我們</a></div></div><div id="6oc1ux2" class="rightbox"><h3>公司基本資料信息</h3><p style="border:0;"><a rel="nofollow">仙桃市百事德化工有限責(zé)任公司</a></p><p><span>聯(lián)系人：</span>謝進(jìn)濤</p><p><span>郵箱: </span>267304616@qq.com</p><p><span>電話: </span>15852535713</p><p><span>傳真: </span>0510_86380198</p><p><span>網(wǎng)址: </span></p><p><span>手機(jī): </span>0510-86380198</p><p><span>地址: </span>沙嘴街道光湖路8號(hào)</p><p>[當(dāng)前離線] <a rel="nofollow"> [加為商友] </a><a rel="nofollow"> [發(fā)送信件] </a></p></div></div><div id="bzcblgq" class="page-proshow02"><p class="title">詳細(xì)說(shuō)明</p><div id="446x96c" class="box"><p><p> 冷凍干燥，然后煅燒，即得。所述模板劑包括十六烷基三甲溴化銨ctab或十六烷基三甲氯化銨ctac。所述ph調(diào)節(jié)劑包括氟化銨nh4f、三乙醇胺tea或氫氧化鈉naoh。所述硅源包括正硅酸乙酯teos、正硅酸丙酯tpos或正硅酸丁酯tbos。所述攪拌反應(yīng)轉(zhuǎn)速為200～300rpm。所述離心速度為10000～10500rpm，離心時(shí)間為10～15min。所述煅燒的工藝參數(shù)為：升溫速度為1～2℃/min，600℃煅燒5h。煅燒是為了除去msns中的模板劑。所述步驟(1)中刻孔劑包括碳酸鈉、碳酸鉀、碳酸氫鈉或碳酸氫鉀。所述步驟(1)中刻孔劑水溶液濃度為～。所述步驟(1)中攪拌溫度為21～25℃，攪拌時(shí)間為7～9h。所述步驟(1)中攪拌轉(zhuǎn)速為200～300rpm。所述步驟(1)中離心速度為10000～10500rpm，離心時(shí)間為10～15min。所述步驟(1)中洗滌為：用去離子水和無(wú)水乙醇各洗滌三次，鎮(zhèn)江鋁合金常溫?zé)o鎳封孔劑表面活性劑。所述步驟(2)中硒源包括亞硒酸鈉na2seo3或硒酸鈉na2seo4。所述步驟(2)中硒源和抗壞血酸摩爾比為1:3～1:4。所述步驟(2)中反應(yīng)為：出現(xiàn)沉淀后繼續(xù)反應(yīng)15min。所述步驟(3)中煅燒溫度為235℃，煅燒時(shí)間為5h。所述步驟(3)中洗滌為：用去離子水反復(fù)洗滌靜置直到廢液為澄清透明，鎮(zhèn)江鋁合金常溫?zé)o鎳封孔劑表面活性劑。所述步驟(3)中se-msns的se負(fù)載量為5wt，鎮(zhèn)江鋁合金常溫?zé)o鎳封孔劑表面活性劑.％-45wt.％；se-msns粒徑為±。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="鎮(zhèn)江鋁合金常溫?zé)o鎳封孔劑表面活性劑" src="https://tyunfile.71360.com/UploadFile/xtsbsd1/637262913996914063/9599976.png"></div><p> 開(kāi)始生產(chǎn)。鋁合金氧化后，在1#封孔槽內(nèi)，可按2um/min設(shè)計(jì)封孔時(shí)間。封孔完成后，經(jīng)2#和3#水洗槽，清洗鋁合金表面殘留封孔藥液，然后風(fēng)干、包裝，完成生產(chǎn)全過(guò)程。2、封孔槽液過(guò)濾再生操作。經(jīng)過(guò)長(zhǎng)期生產(chǎn)，1#封孔槽液可能出現(xiàn)渾濁，可啟動(dòng)過(guò)濾系統(tǒng)，對(duì)封孔液過(guò)濾再生。操作方法如下：關(guān)閉3#、4#閥門，清洗耐酸泵、過(guò)濾器及管道；開(kāi)啟1#、2#閥門；啟動(dòng)耐酸泵，循環(huán)過(guò)濾1#封孔槽，至清澈見(jiàn)底為止，完成封孔液再生。3、廢水處理操作。封孔生產(chǎn)過(guò)程中，封孔藥劑不斷帶人水洗槽，降低水洗槽的pH值?？蓡?dòng)廢水處理系統(tǒng)，對(duì)水洗液過(guò)濾再生，循環(huán)利用。操作方法如下：關(guān)閉1#、2#閥門，開(kāi)啟3#、4#、5#閥門；啟動(dòng)耐酸泵，將4#沉淀槽的水洗液經(jīng)過(guò)濾器過(guò)濾后，抽至3#水洗槽，然后經(jīng)2#水洗槽，自流回4#沉淀槽，完成水洗槽的循環(huán)過(guò)濾。當(dāng)水洗液的pH值低于，停止耐酸泵，關(guān)閉3#、4#、5#閥門，開(kāi)啟氣攪拌6#閥門，將生石灰加入4#沉淀槽，邊加邊攪拌，邊測(cè)pH值，至pH值接近，停止加藥和攪拌，靜置1小時(shí)，重新啟動(dòng)廢水處理系統(tǒng)。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="鎮(zhèn)江鋁合金常溫?zé)o鎳封孔劑表面活性劑" src="https://tyunfile.71360.com/UploadFile/xtsbsd1/637262913898906250/6931910.png"></div><p> 本發(fā)明還提供一種上述方法制備得到的載硒的介孔二氧化硅納米材料。本發(fā)明還提供一種上述方法制備得到的載硒的介孔二氧化硅納米材料的應(yīng)用。本發(fā)明采用溶膠-凝膠方法制備得到介孔二氧化硅(msns)，并進(jìn)一步利用化學(xué)刻蝕法處理獲得一種較大孔徑的介孔二氧化硅，然后通過(guò)超聲輔助-熔融滲透方法(ultrasonicationassisted-meltinfiltration，ua-mi)負(fù)載高量納米硒(se)，超聲條件下將抗壞血酸溶液迅速滴加入硒源和擴(kuò)孔的介孔二氧化硅溶液中反應(yīng)，得到混合溶液，然后將混合溶液冷凍干燥，煅燒，這樣可以使納米se充分填充在孔道內(nèi)，從而負(fù)載高量納米硒，由于納米se充分填充在孔道內(nèi)，可達(dá)到緩慢持久的釋放效果。本發(fā)明制備的擴(kuò)孔的msns平均孔徑和孔容分別為，將其作為載體負(fù)載納米硒se得到的se-msns，其中含硒量比較高可達(dá)45wt.％，且負(fù)載量在5wt.％-45wt.％可精確調(diào)控，粒徑為119±4nm。本發(fā)明中se-msns功能單元結(jié)構(gòu)穩(wěn)定、尺寸可控、具有良好的分散性，更重要的是可以利用更少量的msns負(fù)載更多量的se，提高了納米se的負(fù)載率和msns的利用率。有益效果本發(fā)明獲得的se-msns具有載硒量高、可調(diào)控性強(qiáng)，分散性好，顆粒均一，se可以充分填充在msns的孔道中。相較于純se。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="鎮(zhèn)江鋁合金常溫?zé)o鎳封孔劑表面活性劑" src="https://tyunfile.71360.com/UploadFile/xtsbsd1/637262913937138672/5901259.png"></div></p><br /><p>文章來(lái)源地址: 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