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#f30;"></span></p><p><span>產(chǎn)品關(guān)鍵詞：</span>無鎳封孔劑分析</p><p><span>***更新：</span>2020-06-11 07:24:04</p><p><span id="click" >瀏覽次數(shù)：0次</span></p><a rel="nofollow" class="button">聯(lián)系我們</a></div></div><div id="7ua8xg2" class="rightbox"><h3>公司基本資料信息</h3><p style="border:0;"><a rel="nofollow">仙桃市百事德化工有限責(zé)任公司</a></p><p><span>聯(lián)系人：</span>謝進(jìn)濤</p><p><span>郵箱: </span>267304616@qq.com</p><p><span>電話: </span>15852535713</p><p><span>傳真: </span>0510_86380198</p><p><span>網(wǎng)址: </span></p><p><span>手機(jī): </span>0510-86380198</p><p><span>地址: </span>沙嘴街道光湖路8號</p><p>[當(dāng)前離線] <a rel="nofollow"> [加為商友] </a><a rel="nofollow"> [發(fā)送信件] </a></p></div></div><div id="lodgkuc" class="page-proshow02"><p class="title">詳細(xì)說明</p><div id="yrmx7v7" class="box"><p><p> 開始生產(chǎn)。鋁合金氧化后，在1#封孔槽內(nèi)，可按2um/min設(shè)計(jì)封孔時(shí)間。封孔完成后，經(jīng)2#和3#水洗槽，清洗鋁合金表面殘留封孔藥液，然后風(fēng)干、包裝，完成生產(chǎn)全過程。2、封孔槽液過濾再生操作。經(jīng)過長期生產(chǎn)，無鎳封孔劑分析，1#封孔槽液可能出現(xiàn)渾濁，可啟動過濾系統(tǒng)，對封孔液過濾再生。操作方法如下：關(guān)閉3#、4#閥門，清洗耐酸泵、過濾器及管道；開啟1#、2#閥門；啟動耐酸泵，循環(huán)過濾1#封孔槽，至清澈見底為止，完成封孔液再生。3、廢水處理操作。封孔生產(chǎn)過程中，封孔藥劑不斷帶人水洗槽，降低水洗槽的pH值。可啟動廢水處理系統(tǒng)，對水洗液過濾再生，循環(huán)利用。操作方法如下：關(guān)閉1#、2#閥門，開啟3#、4#、5#閥門；啟動耐酸泵，將4#沉淀槽的水洗液經(jīng)過濾器過濾后，抽至3#水洗槽，然后經(jīng)2#水洗槽，自流回4#沉淀槽，完成水洗槽的循環(huán)過濾。當(dāng)水洗液的pH值低于，停止耐酸泵，關(guān)閉3#、4#、5#閥門，無鎳封孔劑分析，開啟氣攪拌6#閥門，將生石灰加入4#沉淀槽，邊加邊攪拌，邊測pH值，無鎳封孔劑分析，至pH值接近，停止加藥和攪拌，靜置1小時(shí)，重新啟動廢水處理系統(tǒng)。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="無鎳封孔劑分析" src="https://tyunfile.71360.com/UploadFile/xtsbsd1/637262913898906250/6931910.png"></div><p> 1)msns的介孔孔道可進(jìn)一步利用化學(xué)刻蝕劑反應(yīng)，擴(kuò)大孔徑；(2)利用se的低熔點(diǎn)性(217℃)及msns較大的介孔結(jié)構(gòu)，在一定溫度下，使熔融態(tài)se借助流動性和虹吸效應(yīng)灌注到msns的介孔結(jié)構(gòu)中，將se單質(zhì)均勻地填充到msns的孔道中并調(diào)節(jié)其負(fù)載量，有效地利用了msns介孔結(jié)構(gòu)的優(yōu)勢，提高se的負(fù)載率。本發(fā)明提供一種載硒的介孔二氧化硅納米材料的制備方法，包括：(1)將介孔二氧化硅msns與刻孔劑水溶液混合，攪拌，離心，洗滌，冷凍干燥，得到擴(kuò)孔的介孔二氧化硅；其中msns與刻孔劑質(zhì)量比為～；(2)將硒源與步驟(1)中擴(kuò)孔的介孔二氧化硅加入到水中，將抗壞血酸加入到水中，超聲條件下將得到的抗壞血酸溶液迅速滴加入得到的硒源和擴(kuò)孔的介孔二氧化硅溶液中反應(yīng)，得到混合溶液，其中混合溶液中擴(kuò)孔的介孔二氧化硅濃度為5mg/ml～10mg/ml，硒源濃度為30mmol/l～60mmol/l，抗壞血酸濃度為45mmol/l～137mmol/l；(3)將步驟(2)中混合溶液冷凍干燥，然后煅燒，洗滌，離心，冷凍干燥，得到載硒的介孔二氧化硅納米材料se-msns。所述步驟(1)中介孔二氧化硅msns的制備方法包括：將模板劑和ph調(diào)節(jié)劑溶解于水中，在80℃攪拌反應(yīng)50min～70min，滴加入硅源，繼續(xù)反應(yīng)50min～70min，冷卻至室溫，離心。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="無鎳封孔劑分析" src="https://tyunfile.71360.com/UploadFile/xtsbsd1/637262913937138672/5901259.png"></div><p> 封孔質(zhì)量提高；但pH值太高，型材表面容易產(chǎn)生白灰，這主要是因?yàn)榉佀崾シ€(wěn)定性，大量水解；pH值太低，不足以造成氟鈦酸水解，達(dá)不到封孔效果。pH值對封孔的作用原理是按（2）（3）（4）式的化學(xué)反應(yīng)，氟鈦酸的水解，氟與氧化膜的反應(yīng)，微孔中pH值的上升，膜孔中生成的Ti(OH)4沉積來達(dá)到封孔的目的，而水解物沉積量的多少直接影響封孔的效果。pH值在，可達(dá)到封孔的目的；pH值在比較好，這時(shí)的酸度正好在氟鈦酸的水解平衡區(qū)間。（4）氟鈦酸濃度對封孔質(zhì)量的影響本發(fā)明選用氟鈦酸作為主封孔物質(zhì)，氟鈦酸根是封孔槽液中**主要的離子之一。封孔是通過氟鈦酸根進(jìn)入氧化膜孔進(jìn)行水解沉淀得以實(shí)現(xiàn)的，氟鈦酸體系無鎳快速封孔的機(jī)理是水解-溶解-沉積反應(yīng)，其封孔物質(zhì)主要由Ti(OH)4和Al2(OH)3F3組成，是按（1）~（5）式反應(yīng)的綜合結(jié)果。Ti(OH)4填充速度直接影響封孔速度，氟鈦酸含量對封孔質(zhì)量影響很大。實(shí)驗(yàn)結(jié)果表明氟鈦酸（50wt.%）濃度控制在。（5）緩蝕劑濃度對封孔質(zhì)量的影響本發(fā)明緩蝕劑選用低分子多元醇類，如乙二醇、丙三醇和山梨醇等，由帶負(fù)電的羥基吸附在帶正電荷的鋁合金表面，隔離槽液，減緩腐蝕。氟鈦酸封孔體系下，pH值工作區(qū)間，偏酸性，按（4）（5）式。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="無鎳封孔劑分析" src="https://tyunfile.71360.com/UploadFile/xtsbsd1/637262913996914063/9599976.png"></div></p><br /><p>文章來源地址: http://www.cdcfah.com/cp/222779.html</p></div></div></div></div></div><div id="cjkvv3j" 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