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href="http://www.cdcfah.com/cp/third-jxhxp_qitazhuji/">其他助劑</a>?泰州生產(chǎn)封孔劑封閉劑仙桃市百事德化工供應(yīng)</p><div id="xhr97rr" class="leftbox clearfix"><h1>泰州生產(chǎn)封孔劑封閉劑仙桃市百事德化工供應(yīng)</h1><div id="jvzdxt9" class="proBig"><div id="bndjxhf" class="bigimg"><div><p class="pic"><img src="https://tyunfile.71360.com/UploadFile/xtsbsd1/637262913898906250/6931910.png" class="vcenter" onerror="javascript:this.src='/static/new_net_01/images/nopic.jpg';"></p></div></div><div id="blfjthd" class="smallimg"><div><p class="pic"><img src="https://tyunfile.71360.com/UploadFile/xtsbsd1/637262913898906250/6931910.png" class="vcenter" onerror="javascript:this.src='/static/new_net_01/images/nopic.jpg';"></p></div></div></div><div id="fxjfdzd" class="content"><p><span>需求數(shù)量：</span>0</p><p><span>價(jià)格要求：</span>面議</p><p><span>所在地：</span>湖北省</p><p><span>包裝要求：</span><span style="color: #f30;"></span></p><p><span>產(chǎn)品關(guān)鍵詞：</span>泰州生產(chǎn)封孔劑封閉劑</p><p><span>***更新：</span>2020-06-18 14:29:12</p><p><span id="click" >瀏覽次數(shù)：0次</span></p><a rel="nofollow" class="button">聯(lián)系我們</a></div></div><div id="fh7bthl" class="rightbox"><h3>公司基本資料信息</h3><p style="border:0;"><a rel="nofollow">仙桃市百事德化工有限責(zé)任公司</a></p><p><span>聯(lián)系人：</span>謝進(jìn)濤</p><p><span>郵箱: </span>267304616@qq.com</p><p><span>電話: </span>15852535713</p><p><span>傳真: </span>0510_86380198</p><p><span>網(wǎng)址: </span></p><p><span>手機(jī): </span>0510-86380198</p><p><span>地址: </span>沙嘴街道光湖路8號(hào)</p><p>[當(dāng)前離線] <a rel="nofollow"> [加為商友] </a><a rel="nofollow"> [發(fā)送信件] </a></p></div></div><div id="7bx7plb" class="page-proshow02"><p class="title">詳細(xì)說(shuō)明</p><div id="9xl7d7x" class="box"><p><p> 本發(fā)明還提供一種上述方法制備得到的載硒的介孔二氧化硅納米材料。本發(fā)明還提供一種上述方法制備得到的載硒的介孔二氧化硅納米材料的應(yīng)用。本發(fā)明采用溶膠-凝膠方法制備得到介孔二氧化硅(msns)，泰州生產(chǎn)封孔劑封閉劑，并進(jìn)一步利用化學(xué)刻蝕法處理獲得一種較大孔徑的介孔二氧化硅，然后通過(guò)超聲輔助-熔融滲透方法(ultrasonicationassisted-meltinfiltration，ua-mi)負(fù)載高量納米硒(se)，超聲條件下將抗壞血酸溶液迅速滴加入硒源和擴(kuò)孔的介孔二氧化硅溶液中反應(yīng)，得到混合溶液，然后將混合溶液冷凍干燥，煅燒，這樣可以使納米se充分填充在孔道內(nèi)，從而負(fù)載高量納米硒，由于納米se充分填充在孔道內(nèi)，可達(dá)到緩慢持久的釋放效果。本發(fā)明制備的擴(kuò)孔的msns平均孔徑和孔容分別為，將其作為載體負(fù)載納米硒se得到的se-msns，泰州生產(chǎn)封孔劑封閉劑，其中含硒量比較高可達(dá)45wt.％，且負(fù)載量在5wt.％-45wt.％可精確調(diào)控，粒徑為119±4nm，泰州生產(chǎn)封孔劑封閉劑。本發(fā)明中se-msns功能單元結(jié)構(gòu)穩(wěn)定、尺寸可控、具有良好的分散性，更重要的是可以利用更少量的msns負(fù)載更多量的se，提高了納米se的負(fù)載率和msns的利用率。有益效果本發(fā)明獲得的se-msns具有載硒量高、可調(diào)控性強(qiáng)，分散性好，顆粒均一，se可以充分填充在msns的孔道中。相較于純se。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="泰州生產(chǎn)封孔劑封閉劑" src="https://tyunfile.71360.com/UploadFile/xtsbsd1/637262913898906250/6931910.png"></div><p> 抗壞血酸，十六烷基三甲溴化銨(ctab，國(guó)藥集團(tuán)工業(yè)股份有限公司)，氟化銨(nh4f，國(guó)藥集團(tuán)工業(yè)股份有限公司)，正硅酸乙酯(teos，國(guó)藥集團(tuán)工業(yè)股份有限公司)，通過(guò)該制備方法合成載se量30wt.％的se-msns。其具體步驟為：稱取、，隨后加入250ml去離子水，反應(yīng)溫度80℃，充分?jǐn)嚢?h，轉(zhuǎn)子轉(zhuǎn)速控制在200～300rpm；反應(yīng)1h后，向反應(yīng)體系中逐滴加入，繼續(xù)反應(yīng)1h后，冷卻至室溫將樣品離心，將沉淀冷凍干燥得到的白色粉末置于馬弗爐600℃煅燒5h，除去msns中的ctab；稱取，得到濃度為；攪拌條件下將，轉(zhuǎn)速控制在200～300rpm，溫度控制在21～25℃，時(shí)間保持在8h，10000～10500rpm離心后用去離子水和無(wú)水乙醇洗滌三次，冷凍干燥離心后的沉淀產(chǎn)物，得到擴(kuò)孔的msns。稱取，記為a液；稱取，記為b液；充分?jǐn)嚢?轉(zhuǎn)速控制在200～300rpm)使其全部溶于去離子水中；超聲條件下，將b液用注射器迅速滴加到a液，待反應(yīng)液出現(xiàn)紅色物質(zhì)后繼續(xù)反應(yīng)15min，記為c液；將c液冷凍干燥，然后將產(chǎn)物置于馬弗爐235℃煅燒5h，用去離子洗滌至廢液為澄清透明，將沉淀冷凍干燥得到紅色粉末30wt.％se-msns。實(shí)施例2通過(guò)該制備方法合成載硒量20wt.％的se-msns。其具體步驟為：擴(kuò)孔的msns制備方法與實(shí)施例1相同。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="泰州生產(chǎn)封孔劑封閉劑" src="https://tyunfile.71360.com/UploadFile/xtsbsd1/637262913996914063/9599976.png"></div><p> 包括將陽(yáng)極氧化處理未封孔金屬表面貼合的隔離層去除后在平板打印機(jī)上進(jìn)行印刷，待印刷完成后進(jìn)行封孔處理。推薦地，在平板打印機(jī)上對(duì)陽(yáng)極氧化處理未封孔金屬進(jìn)行印刷時(shí)，平板打印機(jī)加熱至20-60攝氏度。上述提供的該可長(zhǎng)期儲(chǔ)存陽(yáng)極氧化未封孔金屬印刷材料在實(shí)際應(yīng)用時(shí)采用加熱平板打印機(jī)，并對(duì)溫度進(jìn)行設(shè)定，是用于通過(guò)將金屬印刷材料放置在平板打印機(jī)進(jìn)行印刷時(shí)，通過(guò)利用將溫度保持在一定溫度環(huán)境下，不僅能夠促進(jìn)噴灑出的墨水快速得到吸收，在保證了墨水吸收效率的同時(shí)，也保證了吸收質(zhì)量，實(shí)現(xiàn)了印刷的性、完整性及高質(zhì)量性。推薦地，封孔處理包括熱封閉處理，推薦地，熱封閉處理包括沸水封閉處理、水解鹽封閉處理和常溫封閉處理中的一種或多種。本發(fā)明的有益效果為：本發(fā)明提供了一種可長(zhǎng)期儲(chǔ)存陽(yáng)極氧化未封孔金屬印刷材料的制備方法，該材料的制備方法中通過(guò)在經(jīng)過(guò)陽(yáng)極氧化處理后未封孔的金屬材料上利用覆膜設(shè)備貼合隔離層，利用隔絕空氣的方法，不僅有效解決了大氣中所含的物質(zhì)污染、氧化上述金屬材料的問(wèn)題，而且地延長(zhǎng)了經(jīng)陽(yáng)極氧化處理后的金屬材料上的微孔閉合所需時(shí)長(zhǎng)，避免了在前期加工過(guò)程中出現(xiàn)污染痕跡的發(fā)生，實(shí)現(xiàn)了能夠進(jìn)行后期深加工的操作。</p></p><br /><p>文章來(lái)源地址: http://www.cdcfah.com/cp/302851.html</p></div></div></div></div></div><div id="b79b9bj" class="page-right twoColRt"><div id="vzdb9pl" class="box01 margin10 clearfix"><h3><a 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