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rel="nofollow" class="button">聯(lián)系我們</a></div></div><div id="h5zbtlh" class="rightbox"><h3>公司基本資料信息</h3><p style="border:0;"><a rel="nofollow">仙桃市百事德化工有限責任公司</a></p><p><span>聯(lián)系人：</span>謝進濤</p><p><span>郵箱: </span>267304616@qq.com</p><p><span>電話: </span>15852535713</p><p><span>傳真: </span>0510_86380198</p><p><span>網(wǎng)址: </span></p><p><span>手機: </span>0510-86380198</p><p><span>地址: </span>沙嘴街道光湖路8號</p><p>[當前離線] <a rel="nofollow"> [加為商友] </a><a rel="nofollow"> [發(fā)送信件] </a></p></div></div><div id="bhdhb5f" class="page-proshow02"><p class="title">詳細說明</p><div id="dxjhtd3" class="box"><p><p> 按照實施例1的方法對鋁合金進行封孔，得到封孔鋁合金件b3。實施例4按照表1列出的組分制備鋁合金陽極氧化膜封孔劑；制備鋁合金陽極氧化膜封孔劑：將鉬酸銨、磷酸鈉、碘化鉀、氯化鑭，鋁材封孔劑使用方法、硅烷偶聯(lián)劑和十二烷基苯磺酸鈉溶于水形成鋁合金陽極氧化膜封孔劑a4。所述鉬酸鈉的含量為4g/l，磷酸鈉的含量為，碘化鉀的含量為4g/l，氯化鑭的含量為，鋁材封孔劑使用方法，γ-(2,3-環(huán)氧丙氧)丙基三甲氧基硅烷的含量為，十二烷基苯磺酸鈉的含量為；按照實施例1的方法對鋁合金進行封孔，得到封孔鋁合金件b4。實施例5按照表1列出的組分制備鋁合金陽極氧化膜封孔劑；制備鋁合金陽極氧化膜封孔劑：將鉬酸鈉、三聚磷酸鈉、碘化鈉、氧化鑭，鋁材封孔劑使用方法、硅烷偶聯(lián)劑和十二烷基苯磺酸鈉溶于水形成鋁合金陽極氧化膜封孔劑a5。所述鉬酸鈉的含量為，三聚磷酸鈉的含量為，碘化鈉的含量為3g/l，氧化鑭的含量為，γ-(2,3-環(huán)氧丙氧)丙基三甲氧基硅烷的含量為，十二烷基苯磺酸鈉的含量為；按照實施例1的方法對鋁合金進行封孔，得到封孔鋁合金件b5。實施例6按照表1列出的組分制備鋁合金陽極氧化膜封孔劑；制備鋁合金陽極氧化膜封孔劑：將鉬酸鈉、三聚磷酸鈉、碘化鉀、氯化鑭、硅烷偶聯(lián)劑和十二烷基苯磺酸鈉溶于水形成鋁合金陽極氧化膜封孔劑a6。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="鋁材封孔劑使用方法" src="https://tyunfile.71360.com/UploadFile/xtsbsd1/637262913937138672/5901259.png"></div><p> 本發(fā)明還提供一種上述方法制備得到的載硒的介孔二氧化硅納米材料。本發(fā)明還提供一種上述方法制備得到的載硒的介孔二氧化硅納米材料的應用。本發(fā)明采用溶膠-凝膠方法制備得到介孔二氧化硅(msns)，并進一步利用化學刻蝕法處理獲得一種較大孔徑的介孔二氧化硅，然后通過超聲輔助-熔融滲透方法(ultrasonicationassisted-meltinfiltration，ua-mi)負載高量納米硒(se)，超聲條件下將抗壞血酸溶液迅速滴加入硒源和擴孔的介孔二氧化硅溶液中反應，得到混合溶液，然后將混合溶液冷凍干燥，煅燒，這樣可以使納米se充分填充在孔道內(nèi)，從而負載高量納米硒，由于納米se充分填充在孔道內(nèi)，可達到緩慢持久的釋放效果。本發(fā)明制備的擴孔的msns平均孔徑和孔容分別為，將其作為載體負載納米硒se得到的se-msns，其中含硒量比較高可達45wt.％，且負載量在5wt.％-45wt.％可精確調控，粒徑為119±4nm。本發(fā)明中se-msns功能單元結構穩(wěn)定、尺寸可控、具有良好的分散性，更重要的是可以利用更少量的msns負載更多量的se，提高了納米se的負載率和msns的利用率。有益效果本發(fā)明獲得的se-msns具有載硒量高、可調控性強，分散性好，顆粒均一，se可以充分填充在msns的孔道中。相較于純se。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="鋁材封孔劑使用方法" src="https://tyunfile.71360.com/UploadFile/xtsbsd1/637262913898906250/6931910.png"></div><p> se-msns顆粒在分散度方面有明顯的優(yōu)勢，因此se-msns具有長效釋放，持久等特點，對金黃色葡萄球菌(，atcc6538)有良好的作用，同時，se-msns材料經(jīng)過兩次回收后率依然達到100％，可作為一種可重復使用的長效材料。本發(fā)明工藝簡單，可控性強，成本低。附圖說明圖1為實施例1-4中不同含se量的se-msns在不同ph下的釋放曲線，其中(a)ph＝；(b)ph＝。圖2為實施例1-4中未刻蝕msns和刻蝕msns的氮氣等溫吸脫附曲線(a)和bjh模型孔徑分布圖(b)。圖3為實施例1-4中不同載se量se-msns的場發(fā)射掃描電鏡圖，其中(a)載se量為30wt.％，(b)載se量為35wt.％，(c)載se量為40wt.％，(d)載se量為45wt.％。圖4為實施例1-2和4-5中不同含se量的se-msns樣品的xrd圖。圖5為實施例1和3-4中不同含se量的se-msns和純se(a)、次回收的實施例3中se-msns和純se(b)、第二次回收的實施例3中se-msns(c)對作用圖。具體實施方式下面結合具體實施例，進一步闡述本發(fā)明。應理解，這些實施例*用于說明本發(fā)明而不用于限制本發(fā)明的范圍。此外應理解，在閱讀了本發(fā)明講授的內(nèi)容之后，本領域技術人員可以對本發(fā)明作各種改動或修改，這些等價形式同樣落于本申請所附權利要求書所限定的范圍。實施例1選擇分析純的亞硒酸鈉。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="鋁材封孔劑使用方法" src="https://tyunfile.71360.com/UploadFile/xtsbsd1/637262913996914063/9599976.png"></div></p><br /><p>文章來源地址: http://www.cdcfah.com/cp/99251.html</p></div></div></div></div></div><div id="xrbxzt3" class="page-right twoColRt"><div id="hb5nzvr" 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